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National Repository of Grey Literature

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	Studium biodegradovatelných směsí škrob/polykaprolakton metodami NMR spektroskopie pevného stavu Spěváček, Jiří ; Brus, Jiří ; Divers, T. ; Grohens, Y. 1H relaxation times T1(H) and T1.rho.(H) were measured via 13C detection on starch/polycaprolactone (PCL) and starch formate/PCL blends to characterize their morphology (domain size). From the results it follows that while blends starch/PCL are phase-separated on the scale 20-110 nm, starch formate/PCL blend is homogeneously mixed on this scale. Therefore formylation of starch significantly improves its miscibility with PCL. Detailed record
	Determination of polysaccharides structure by spectroscopic methods Synytsya, A. ; Blafková, P. ; Čopíková, J. ; Spěváček, Jiří Possibilities of vibrational and NMR spectroscopy in structural characterization of polysaccharides were illustrated on examples of several polysaccharide systems (pectins, chitin, chitosan, chitosan lactate, carrageens, chondroitinsulphate). Detailed record
	Structural characterization of chitin/glucan complexes from the mushroom Pleurotus sp. and Aspergillus niger mycelium Spěváček, Jiří ; Synytsya, A. ; Brus, Jiří ; Ederová, J. ; Čopíková, J. Structure and composition of insoluble chitin/glucan complexes isolated from the mushroom Pleurotus spstructure, solid state NMR and Aspergillus niger mycelium were characterized by a combination of solid-state 13C NMR spectroscopy, IR spectroscopy and thermal methods. Detailed record
	Structure characterization of glucanes by 13C NMR spectroscopy Spěváček, Jiří The principles of high resolution solid state 13C NMR spectroscopy are explained in this contribution. Some possibilities of this method in the structural characterization of glucans and their derivatives are demonstrated on examples of cellulose, chitin, chitosan and chitin/glucan complexes. Detailed record

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