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WP5 Status Report Months 31 to 50
Křišťál, Jiří ; Stavárek, Petr ; Jiřičný, Vladimír
Within WP5 in this reporting period focused on the development of a new intensified reactor concept for sulph(on)ation reaction. Based on the previous hydrodynamic experiments and mathematical models we designed a new reactor – microSulphonator. We also constructed and manufactured several prototypes that were later tested with model fluids. Experimental data were used for the validation of the models defined previously. Results of this period served as a basis for the final microSulphonators to be tested in the PGB pilot plant during the demonstration phase of the F3 project.
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Project Report Beneficiary No.17 ICPF Reporting period: Months 13 to 24 (01 June 2010 to 31 May 2011)
Křišťál, Jiří ; Stavárek, Petr ; Jiřičný, Vladimír
To assess the commercially available SO2 oxidation catalyst and select several for further testing we performed the extensive literature review. Based on that, we tested the selected catalysts for SO2 oxidation in experiments with the KIT lab microreactor, and started the detailed catalyst comparison based on the evaluation of the pre-exponential factor (A0) and activation energy (EA) calculated from the kinetic model by fitting the experimental data. To verify the possible design of a new sulph(on)ation reactor we performed the initial hydrodynamic experiments with gas-liquid two-phase flow in small channels.
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