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Establishment of the method for determination of selected congeners of polychlorinated biphenyls in water using GC-ECD
TALAVÁŇOVÁ, Eliška
This bachelor thesis deals with the determination of selected congeners of polychlorinated biphenyls in water using GC-ECD. Firstly, the development and optimisation of the analytical method was performed. The following parameters of the analytical method were chosen for optimization: carrier gas flow rate, sample volume, injector temperature, splitless time, initial column temperature, temperature gradient and detector temperature. Then, extraction time of the liquid-liquid extraction was optimised. Finally, the method was successfully validated and applied to the analysis of a real tap water sample.

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2 Talaváňová, Eva
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