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Use of X-ray diffraction analysis in the optimization of cathode material syntheses for Li-ion batteries
Kunz, Marek ; Čech, Ondřej (referee) ; Chladil, Ladislav (advisor)
This thesis deals with study of structural changes in electrode materials prepared by spray-dry synthesis at different calcination temperatures using X-ray diffraction analysis. In the theoretical part, the work deals with the principle of XRD, parameters that influence the resulting diffractogram and Rietveld analysis. The part further deals with possible syntheses of cathode materials, calcination, and possible ways of battery degradation. The experimental part focuses on investigating the ideal calcination temperature and time of prepared cathode material samples.

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