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Gel polymer electrolytes with fire retardands
Veselkova, Iuliia ; Jahn, Michal (referee) ; Sedlaříková, Marie (advisor)
This graduate work deals with the study and preparation of gel polymer electrolytes with flame retardants for lithium-ion batteries. The theoretical part describes the types of electrolytes, their features, benefits, how they differ and where they are used in detail. The basis of this section is gel electrolytes with flame retardants, to measure their electrical and electrochemical properties. The experimental part deals with the preparation of samples of gel electrolytes with different percentages of flame retardant, where varied species of flame retardants and measuring their electrical conductivity and potential windows. Impedance spectroscopy, cyclic voltammetry and dynamic-analytical thermal analysis were selected as measuring methods.
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Using thermochromic systems for testing heat distribution
Klimeš, Jan ; Sedlaříková, Marie (referee) ; Zatloukal, Miroslav (advisor)
This thesis deals with principles of thermochromism and its possible applications in heat distribution testing. Theoretical part describes mechanisms which allow the thermochromic properties of the substances. Particular attention is paid to cholesteric liquid crystals. Ability to measure the heat for this type of liquid crystals was varified. Also long service life in high humidity environment, enviroment with intense UV radiation, cyclic changes in temperature or immersion in water was tested. A possibility of their practical use in diagnosis was verified as well. Specifically mapping of heat distribution on an assembled PCB. Conclusion contains comparison and evaluation of this method in terms of accuracy, user comfort and economic advantages compared to conventional infrared sensors.
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Gel polymer electrolytes with nanoparticles
Szotkowski, Radek ; Sedlaříková, Marie (referee) ; Jahn, Michal (advisor)
This master‘s thesis concerns gel polymer electrolytes formed on a methyl methacrylate base with selected types of nanoparticles. In the thesis are also analyzed the methods for measuring electrochemical properties. The practical portion deals with sample preparations of gel polymer electrolytes with different contents of alkaline salt in a solvent, creating gels with different nanoparticle content and comparing gel polymer electrolytes polymerized with heat and UV radiation. The thesis deals with the evaluation of these samples from the viewpoint of electrical conductivity and potential windows as well as thermal analysis of selected samples.
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New gel electrolytes
Sumka, Martin ; Jahn, Michal (referee) ; Sedlaříková, Marie (advisor)
This master´s thesis deals with the properties of gel polymer electrolytes, brief characteristics of other types of electrolytes and materials that are used for preparing polymer electrolytes. The thesis explains the use of the gel electrolytes in practice, the current conduction in the electrolytes and the properties of ionic liquids, and flame retardants. This thesis also focuses on methods of measurement of mechanical properties of gel polymer electrolytes. The practical part is focused on preparation of methacrylate gel electrolytes and their modifications with the use of flame retardant - triethyl phosphate (TEP) and ionic liquid - 1-ethyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide (Emim TFSI). In this part there are evaluations of their potential funcionality (potential window) and specific conductance conductivity using the method LSV (linear sweep voltammetry) and impedance spectroscopy. The practical part also includes a thermal analysis of selected samples by TGA, DTA and EGA methods.
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Bones implants based on Fe
Hávová, Mariana ; Vondrák, Jiří (referee) ; Sedlaříková, Marie (advisor)
This thesis refers to Fe-based biodegradable materials and their potencial aplications in medicine, especially as temporary bone implants. This work generaly summaries aplications of biomaterial in medicine with more interest kept on biodegradable materials and their in-vivo corrosion. The experimental part refers to conduction of porous Fe-based materials with silica addition. The structure of prepared specimens is identified by EDX and XRD analysis. The imersion test and electrochemical studies were conducted to observe corrosion behaviour with respect to different concentration of silica. Potenciodynamic curves were obtained to determine corrosion potencial and corrosion current density of prepared samples.
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Ionic liquids for electrochemical power sourcees
Korec, Pavol ; Máca, Josef (referee) ; Sedlaříková, Marie (advisor)
Bachelor thesis Ionic liquids for electrochemical power sources deals with the measurement of electrical properties of ionic liquids, their conductivity and potential window, to broaden the knowledge of their optional use as lithium – ion battery electrolytes. The theoretical section of the work deals with the properties and usage of ionic liquids, structure and functionality of lithium – ion batteries and measurment of electrochemical impedance spectroscopy a cyclic voltammetry. The practical section of the work describes the process of measuring the conductivity and potential window of ionic liquids, observes the changes made to the electrical properties of the samples by adding LiBF4 salt and propylencarbonate solvent and summarizes results.
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Biodegradable metal materials for bone tissue prosthetics
Panáková, Olga ; Vondrák, Jiří (referee) ; Sedlaříková, Marie (advisor)
This paper is focused on use of metal materials as a bone replacement. For coherence of this text is necessary theoretical preamble which is consisting of describing metal properties, aimed particularly at corrosion, valuation methods of disposition to corrosion and mainly corrosion itself. This paper also includes description of techniques of preparation, which involves selection of material and its procession. Furthermore there are stated results of experiments. Those are amended with pictures.
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Bone implants based on Fe
Bachmayer, Marek ; Vondrák, Jiří (referee) ; Sedlaříková, Marie (advisor)
This thesis deals with usage of metal materials in bone implats creation process. This work also includes information about structure and attributes of bones, body fluids and content of iron in human organism. Following part of the paper deals with osteosynthesis, therefore commonly used methods of treating bone defects. Next part of this bachelor’s thesis is discussing the issue of biomaterials, biocompatibility and biodegradability of metal materials. Sample preparion procedure and description of samples, electrochemical corrosion and microscopic observation is included altogether with a pictorial documentation at the last chapters of this paper.
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