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Tungsten trioxide coatings fabricated from nanocrystalline suspension and binder
Filipská, Markéta ; Zlámal,, Martin (referee) ; Dzik, Petr (advisor)
This diploma thesis deals with layers of tungsten oxide, which are prepared from a nanoparticle suspension and a binder. The coating composition consisted in the first case of ground tungsten oxide nanoparticles alone, then of acetylated peroxotungstic acid alone and finally of a mixture of ground tungsten oxide mixed with acetylated peroxotungstic acid. The compositions thus formed were applied to conductive FTO glass and thus act as photoanodes. A stainless steel needle is used as a counter electrode for volt-ampere measurements. The work focuses on the study of physicochemical properties of prepared photoanodes and their optimalization in order to obtain the highest possible values of generated photocurrents. The electrical properties of all cells were determined using voltammetric characteristics.
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Electroassisted photocatalysis
Filipská, Markéta ; Pekárková, Jana (referee) ; Dzik, Petr (advisor)
This thesis is focused on fotoelectrochemical cells, where as photocathode is used titanium dioxide coated on conductive FTO glass and as counter electrode is used gold electrode. Thesis is also focused on relationship between intensity of irradiation and Faradaic efficiency and also influence of the overvoltage to the rate of degradation od the model pollutant, in this case Acid Orange 7. Electrical properties were measured by recording values of photocurrent. The aim of this thesis was to study influence material composition of photoanode and connection with intensity of irradiation, rate of degradation proces of model pollutant and current.
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Tungsten trioxide coatings fabricated from nanocrystalline suspension and binder
Filipská, Markéta ; Zlámal,, Martin (referee) ; Dzik, Petr (advisor)
This diploma thesis deals with layers of tungsten oxide, which are prepared from a nanoparticle suspension and a binder. The coating composition consisted in the first case of ground tungsten oxide nanoparticles alone, then of acetylated peroxotungstic acid alone and finally of a mixture of ground tungsten oxide mixed with acetylated peroxotungstic acid. The compositions thus formed were applied to conductive FTO glass and thus act as photoanodes. A stainless steel needle is used as a counter electrode for volt-ampere measurements. The work focuses on the study of physicochemical properties of prepared photoanodes and their optimalization in order to obtain the highest possible values of generated photocurrents. The electrical properties of all cells were determined using voltammetric characteristics.
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Electroassisted photocatalysis
Filipská, Markéta ; Pekárková, Jana (referee) ; Dzik, Petr (advisor)
This thesis is focused on fotoelectrochemical cells, where as photocathode is used titanium dioxide coated on conductive FTO glass and as counter electrode is used gold electrode. Thesis is also focused on relationship between intensity of irradiation and Faradaic efficiency and also influence of the overvoltage to the rate of degradation od the model pollutant, in this case Acid Orange 7. Electrical properties were measured by recording values of photocurrent. The aim of this thesis was to study influence material composition of photoanode and connection with intensity of irradiation, rate of degradation proces of model pollutant and current.
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