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Possibilities of electrochemical generation of volatile compound of gold Průša, Libor ; Hraníček, Jakub (advisor) ; Musil, Stanislav (referee) The possibilities of electrochemical generation of gold volatile compound have been studied in this work. All experiments have been employed in electrochemical continuous flow generation. The previous aim of this work was to investigate if it is possible to generate the volatile form of gold using electrochemical generation of volatile compounds. Lead, platinum and alloy of lead and tin were used as cathode materials. Consequently, optimizations of experimental conditions were carried out. The optimized experimental conditions were: carrier gas flow rate, flow rate of electrolytes, electric current used for electrochemical generation, influence of the different types of gas-liquid separator, atomizer temperature. The calibration and other characteristics were found. At the conclusion, effect of oxygen on the signal intensity was studied. Key words Electrochemical generation of volatile compound atomic absorption spectrometry quartz tube atomizer flow-through electrolytic cell volatile compound gold Detailed record

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