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Quantitative image analysis of precipitates in Ni-rich NiTi shape memory alloys
Bojda, Ondřej ; Dlouhý, Antonín ; Fiala, J.
A microstructure of a Ti-50.7at%Ni shape memory alloy resulting from solution annealing and subsequent aging at 500°C/3.6ks/8MPa is quantitatively analysed. The TEM study is assisted by Adaptive Contrast Control (ACC) routines embedded in a recent image processing system. The assessment focuses on the number density, size and distribution of crystallographic variants of Ni4Ti3 precipitates. It was found that the distribution of crystallographic particle variants in the microstructure is inhomogeneous. The influence of the heterogeneous Ni4Ti3 precipitation on the characteristics of the martensitic transformation B2®B19´ is briefly discussed.

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