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Properties of aprotic electrolytes for lithium-ion accumulators
Staněk, Vladimír ; Máca, Josef (referee) ; Frk, Martin (advisor)
The present work deals with the properties of suitable electrolytes for lithium-ion batteries. The first part described in the current issue of electrolytes for lithium-ion batteries, types of solvents and their properties and methods of measurement properties. The second part is devoted to the measurement of the properties of solvents and electrolytes such as relative permittivity, density and viscosity. Measurement of relative permittivity was focused on the measurement of the solvent mixture with varying the percentage of the solvent. Viscosity and density were measured on a solvent with a lithium salt added (final electrolyte).
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Impact of technological parameters on electrochemical properties of negative electrode in lithium-ion battery
Živčic, Samuel ; Máca, Josef (referee) ; Libich, Jiří (advisor)
This bachelor thesis deals with the issue of li-ion batteries and consists of two main parts. The first part of the thesis deals with a theory. It describes the functionality of electrochemical cells, especially li-ion cells. Operational principle of the cell is discussed, with the main focus given on negative electrode (anode) and the material it consists of, the natural graphite, mainly his electrochemical properties. Last chapter of theory describes expected impact of technological parameters on electrochemical properties of negative electrode. The second part of the thesis is the practical part. First, it describes procedure of making electrodes in laboratory and afterwards it provides an explanation of used measuring methods, steps taken during the measurement, and the results of the measurements. At the end of the thesis, the influence of pressure and layer thickness on electrochemical properties of natural graphite and on capacitive and current characteristics of negative electrode is evaluated.
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The Freezing Point Determination Of Electrolytes With Fire Retardant By Cryoscopy Method
Štulák, Stanislav ; Vondrák, Jiří (referee) ; Máca, Josef (advisor)
The thesis is devoted to the field of properties investigation of new types of electrolytes, and assess the appropriateness of electrolytes studied in this paper for use in Li -ion batteries. It focuses specifically on electrolytes based on aprotic solvents and their mixtures with the flame retardants. The goal of the thesis is to investigate the effects of FRAs on electrolyte mixtures via changes in specific conductivity and freezing point. These objectives were fulfilled by using electrochemical impedance spectroscopy in combination with a cryoscopic measurement method. There were overall 16 samples examined. The samples were prepared as a combination of chemicals, specifically Ethylene carbonate (EC), propylene carbonate (PC), dimethyl carbonate (DMC), dimethyl sulfone (DMSO2), triethyl phosphate (TEP) Dimethyl methylphosphonate (DMMP), triphenyl phosphate (TPP). Based on the results of the experiments, the mixtures were sorted according to the observed properties in the tables listed in the last part of this paper. These values can be further used to supplement the continuing research of electrolytes and also as assistance in searching for the new electrolyte mixtures.
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Expanded Graphite as Negative Electrode for Lithium-Ion Batteries
Bibik, Maria ; Máca, Josef (referee) ; Libich, Jiří (advisor)
This bachelor’s thesis examines the issues related to the lithium-ion batteries and describes their basic elements, operating principle and technological parameters. It is focused on studying different materials for the negative electrode (anode) that is based on natural graphite. It describes in detail expanded natural graphite materials which are used as an active electrode material. This thesis describes experiments of the impact of the pressure force on power and capacity characteristics of the negative electrode in aprotic system of li-ion batteries.
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Negative electrodes for sodium ion batteries
Šátek, Dominik ; Libich, Jiří (referee) ; Máca, Josef (advisor)
This bachelor thesis deals with sodium-ion accumulators with focus on negative electrode, introduces basic terms in the field of secondary cells and describes production of accumulators. The result of this work are tested electrodes based on natural carbon and sodium metatitanate. These electrodes are then compared with each other and evaluated.
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Infuence of Technological Parameters on Electrochemical Properties of Negative Electrode in Lithium-ion Cell
Kaňa, Michal ; Máca, Josef (referee) ; Libich, Jiří (advisor)
This diploma thesis deals with lithium-ion batteries. It is focused on negative electrode on grafit based. The goal of this thesis is to show the problematics of lithium-ion batteries together with possibilities for improvement of their basic parametres as capacity and current elektricity loadability. The first part is focused on the description of functionality of lithiumion battery. The second part is practical and it is focused on production of negative electrodes from natural graphite 280H which has different thickness and compression pressure. The third part describes preparation of negative electrodes from natural graphite 280H and also includes results of measurement. In the last part are different types of negative electrodes from natural graphite 280H compared and evaluated including the determination of conclusions. This comparison and evaluation based on obtained data.
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