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Investigation of deformation mechanisms in textured magnesium alloy by advanced in-situ methods
Dittrich, Jan ; Minárik, Peter (advisor)
Title: Investigation of deformation mechanisms in textured magnesium alloy by advanced in-situ methods Author: Bc. Jan Dittrich Department: Department of Physics of Materials Supervisor: RNDr. Peter Minárik, PhD., Department of Physics of Materials Abstract: This thesis aims to investigate the correlation between texture and the activation of particular deformation mechanisms during the deformation of a rolled magnesium alloy AZ31. A combination of advanced in-situ techniques, providing complementary information about the processes within the material during its deformation, was employed to achieve this goal. The combination of neutron diraction and acoustic emission measurements allowed to investigate both rapid and continuous processes related to changes of the material microstructure resulting from its deformation. The in-situ loading of the sample inside the chamber of a scanning electron microscope, coupled with the electron backscatter diraction analysis, provided more direct observations of the microstructural evolution. Furthermore, the high-speed camera imaging of the deformed sample surface enabled a direct, real-time view of the occurring rapid processes. The results of the experiments conrmed the anisotropy of the mechanical behaviour of samples oriented diversely with respect to the...
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Investigation of deformation mechanisms in textured magnesium alloy by advanced in-situ methods
Dittrich, Jan ; Minárik, Peter (advisor) ; Janeček, Miloš (referee)
Title: Investigation of deformation mechanisms in textured magnesium alloy by advanced in-situ methods Author: Bc. Jan Dittrich Department: Department of Physics of Materials Supervisor: RNDr. Peter Minárik, PhD., Department of Physics of Materials Abstract: This thesis aims to investigate the correlation between texture and the activation of particular deformation mechanisms during the deformation of a rolled magnesium alloy AZ31. A combination of advanced in-situ techniques, providing complementary information about the processes within the material during its deformation, was employed to achieve this goal. The combination of neutron diraction and acoustic emission measurements allowed to investigate both rapid and continuous processes related to changes of the material microstructure resulting from its deformation. The in-situ loading of the sample inside the chamber of a scanning electron microscope, coupled with the electron backscatter diraction analysis, provided more direct observations of the microstructural evolution. Furthermore, the high-speed camera imaging of the deformed sample surface enabled a direct, real-time view of the occurring rapid processes. The results of the experiments conrmed the anisotropy of the mechanical behaviour of samples oriented diversely with respect to the...
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Investigation of deformation mechanisms in textured magnesium alloy
Dittrich, J. ; Čapek, J. ; Knapek, Michal ; Minárik, P.
Advanced in-situ and ex-situ methods were used to reveal active deformation mechanisms during deformation of magnesium alloy with a strong texture. Three sets of samples were prepared from the rolled sheet of commercial AZ31 alloy with respect to its strong basal texture - normal direction (ND), rolling direction (RD) and 45 degrees between RD and ND, and were deformed in both compression and tension. The signal of acoustic emission (AE) was measured concurrently during the deformation. Electron backscattered diffraction (EBSD) was used to study the microstructure after the selected stages of the deformation. It is shown that the extension twinning played an important role during the plastic deformation in the samples having favorably oriented basal texture component, whereas in the unfavorably oriented samples, the role of twinning was marginal. Pronounced activation of twinning only in some samples caused a considerable variation in the deformation behavior and AE response. A consistent link between the energy and amplitudes of the AE signal and the microstructure changes investigated by EBSD was established.
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Investigation of deformation mechanisms in textured magnesium alloy
Dittrich, Jan ; Minárik, Peter (advisor) ; Lukáč, Pavel (referee)
Název práce: Studium deformačních mechanism· v hořčíkové slitině s texturou Autor: Jan Dittrich Katedra: Katedra fyziky materiál· Vedoucí bakalářské práce: RNDr. Peter Minárik, PhD., Katedra fyziky materiál· Abstrakt: Předložená práce se zabývá studiem deformačních mechanism·, zá- visejících na orientaci vzork· v·či p·vodní textuře válcované hořčíkové slitiny, pomocí pokročilých in-situ i ex-situ metod. Během deformačních zkoušek, které byly prováděny v tlaku a v tahu, byla současně zaznamenávána akustická emise. Mikrostruktura deformovaných vzork· poté byla zkoumána metodami optické mi- kroskopie a difrakce zpětně odražených elektron·. V práci byla zjištěna výrazná závislost mechanických vlastností a aktivovaných deformačních mechanism· na orientaci vzork· v·či zjištěné bazální textuře válcovaného plechu hořčíkové sli- tiny AZ31. Dále byla ustanovena souvislost mezi základními parametry akus- tické emise a aktivovanými deformačními mechanismy. Rovněž byla pozorována a objasněna asymetrická odezva akustické emise při deformaci tlakem a tahem, související s rozdílným vývojem mechanického dvojčatění v pr·běhu plastické deformace. Klíčová slova: hořčíkové slitiny, deformace, dvojčatění, akustická emise, EBSD
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