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Characterization and elimination of thermomechanical effects in interferometric length measurement
Řeřucha, Šimon ; Holá, Miroslava ; Lazar, Josef ; Mikel, Břetislav ; Číp, Ondřej
Continuous efforts to develop dimensional measurements at both the nano- and macro-scale continue to present challenges in extending high-precision measurement procedures from the well-controlled experimental environment of a typically single measurement cycle to a constant-load production environment. In the field of laser interferometry, which is both a cornerstone of length metrology in general and an essential part of nanometrology, we have focused on long-term measurement stability (so-called zero-drift) in measurement scenarios and applications based on (mostly laser) interferometry. A well-characterized and compensated measurement zero-drift in such applications becomes more important both with applications in less controlled environments and with increasing measurement timeframes, such as long scans in microscopic nanometrology, long exposures in electron lithography, or interferometric reference calibrations with a larger number of calibration points or repetitions. The goal of the current research effort is to comprehensively investigate error effects and contributions to measurement uncertainty related to zero-drift in laser interferometry-based applications, with a particular focus on temperature effects (as these typically appear to be the dominant contribution) and approaches to suppress them. This effort involves several complementary directions.
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Optical fibre dosimeter
Jelínek, Michal ; Mikel, Břetislav
In the nuclear facility, there is currently a demand for optical methods of measuring gamma radiation. For these measurements, we need very robust measurement methods and sophisticated equipment. Silica optical fibres coupled to crystal scintillators are suitable and we present results from their implementation. The scintillators detect gamma radiation and the silica optical fibres transmit the scintillation light from the scintillator to the detector. We used commercially available silica optical fibres up to 1.5 mm in diameter with different numerical apertures to transmit visible light from the scintillators to the detector.
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Low-temperature emissivity of thin Al2O3 layers deposited on copper substrate
Frolec, Jiří ; Králík, Tomáš ; Nyman, L. ; Pudas, M. ; Kallio, E.
Copper is commonly used in cryogenic systems due to its high thermal and electrical conductivity along with excellent solderability. Very low emissivity values of copper surface also reduce in cryogenic systems heat load transferred by thermal radiation. These values may be, however, enhanced by a prospective coating, deposited usually in order to prevent chemical changes on highly reactive copper surface. This paper focuses on protective layers of Al2O3 with thicknesses up to 28 nm, deposited on polished copper. We measured total hemispherical emissivity at cryogenic temperatures before and after the coating process. Contribution of Al2O3 layer to original copper emissivity increased with rising temperature of the layer and with the layer thickness. However, emissivity of the coated copper stayed below 2%, allowing usage of the coated copper in systems where low heat load by thermal radiation is needed. Preliminary tests with oxygen plasma shows that deposited layers can effectively protect the copper surface against oxidation and maintain the original thermal-radiative properties.
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Optical fibers for measuring ionizing radiation
Jelínek, Michal ; Mikel, Břetislav
Optical fiber ionising radiation measurements cannot be used to continuously measure high-energy ionising radiation, especially gamma radiation. Previously presented sensors and methods use optical fibers with a scintillator on/inside the fiber, optical fibers doped with a scintillator, etc. These methods are not suitable for measuring high-energy radiation mainly due to low efficiency. Therefore, we present a measurement method where optical fibers are used only to transport the scintillation radiation to the shielded detection electronics.
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Multimode optical fiber based endoscopy
Jákl, Petr ; Tučková, Tereza ; Pikálek, Tomáš ; Stibůrek, Miroslav ; Ondráčková, Petra ; Cifuentes, Angel S. ; Šiler, Martin ; Uhlířová, Hana ; Traegaardh, Johanna ; Čižmár, Tomáš
Optical microscopy is a technique for microworld investigation using light waves scattered on particles in sample space. Its main disadvantage in the area of medicine, microbiology and neurology is its low penetration depth - it is very difficult to image structures deeper than approximately 1 mm inside tissue. Conventional endoscopes use refractive or GRIN lens with cross-section of several milimeters in diameter. Therefore, it is necessary to find less invasive probes to perform imaging in living organisms. Favourable alternative is to use multimode optical fiber probe with 100 micrometer diameter. This approach, however, requires advanced shaping of the wavefront in order to achieve diffraction limited imaging.
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An appropriate method for assessing hydrogel pore sizes by cryo-sem
Adámková, Kateřina ; Trudicová, M. ; Hrubanová, Kamila ; Sedláček, P. ; Krzyžánek, Vladislav
The aim of our work was to examine and describe ultrastructure of the agarose hydrogel and any possible structural concentration dependencies, and to assess the distribution and size of pores of agarose hydrogel in dependence on its concentration. Four concentrations were prepared (0.5 %, 1.0 %, 2.0 % and 4.0 % of dry weight content) and cryo-SEM and turbidimetry methods were executed on wet (original) samples in order to image the ultrastructure and measure the pore sizes within. \nReasonable results were obtained for the wet samples as they were closer to their native state they are usually used for applications in. Cryo-SEM and turbidimetry provided comparable results of pore diameters and allowed to compare pore diameters dependant on the concentrations, moreover, it showed more detailed and realistic structure.
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Determination of thickness refinement using STEM detector segments
Skoupý, Radim ; Krzyžánek, Vladislav
Quantitative STEM imaging together with Monte Carlo simulations of electron scattering in solids can bring interesting results about properties of many thin samples. It is possible to determine thickness of a sample, to calculate mass of particles and measure mass per length/area. Appropriate calibration is one of the crucial parts of the method. Even a small error or inaccuracy in detector response to electron beam either blanked or full brings significant error into thickness determination. This problem can be overcome by parallel STEM imaging in more segments of the detector. Comparing more segments gives a possibility to use a signal from different segments for different thicknesses of a sample. Accuracy of individual parts of the detector depends on the captured signal quantity. It is desirable to use such a STEM detector segment that provides the greatest signal change to a unit of thickness. To demonstrate the usage, we used a sample of Latex nanospheres placed on thin carbon lacey film, diameter of the nanospheres was around 600 nm in order to compare the results from different detector segments. Thanks to the known thickness of the sample (calculated from its geometrical shape), it is possible to estimate the optimal acquisition settings and post processing steps with the known and the true state of the sample.
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