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Chemical and microstructural analysis of brick samples from the object of Zákupy castle horse stables
Frankeová, Dita ; Bauerová, Pavla ; Náhunková, Pavla ; Ševčík, Radek ; Mácová, Petra ; Slížková, Zuzana ; Vondráčková, Michaela
As part of the construction-technical survey, historical brick samples were characterized using thermal analysis (TGA), scanning electron microscopy (SEM/EDS), ion chromatography (IC), infrared spectrometry (FTIR) and physical tests. The results of the tests testify to the good production quality of the masonry elements used. Based on the analyzes carried out, it can be assumed that the observed damage to the bricks is caused by high wetting of the masonry in combination with frost cycles, as well as crystallization cycles of water-soluble salts present in the surface layer of some bricks.
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Survey of salinity of masonry under III. courtyard at Prague Castle
Slížková, Zuzana ; Ševčík, Radek ; Viani, Alberto ; Mácová, Petra
Archaeological architectural monuments in the area under III. in the courtyard of Prague Castle were monitored in 2021 in terms of the extent of salt efflorescences and their chemical composition. Salt efflorescence on the marlstone walls of the church of St. Bartholomew contain sodium carbonate and bicarbonate, sodium sulfate and calcium sulfate. Sodium nitrate and potassium nitrate were also present in some samples. The aim of the research is to propose measures to mitigate the effect of salts on the degradation of historic masonry.
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