Národní úložiště šedé literatury Nalezeno 4 záznamů.  Hledání trvalo 0.00 vteřin. 
Metastable iron thin films for magnetic metamaterials
Holobrádek, Jakub ; Man, Ondřej (oponent) ; Urbánek, Michal (vedoucí práce)
Magnetic nanostructures are widely investigated for applications in industrial and fundamental research thanks to their interesting properties. One of the concerned scientific disciplines is magnonics – a novel research topic in magnetism concerned with the physics of spin waves, which can be used for fabrication of novel devices for wave-based computing with low power consumption. Fabrication of magnonic structures by a focused ion beam (FIB) is an alternative method to the commonly used lithographic methods. The material used in this work -- metastable iron – is able to undergo an ion-beam-induced phase transformation from a paramagnetic fcc to a ferromagnetic bcc phase. One of the properties, which affect the spin-wave propagation, is magnetic anisotropy. This thesis presents the influence of UHV conditions during the deposition of the metastable iron film on the magnetic anisotropy of the structures fabricated via FIB into this film. We also investigate the relationship between FIB parameters, crystallographic properties of the resulting structures, and their magnetic anisotropy.
LOW CYCLE FATIGUE BEHAVIOR AND FATIGUE CRACK INITIATION IN MAR-M247 AT 700 °C
Šulák, Ivo ; Obrtlík, Karel ; Hrbáček, K.
The second generation nickel-based superalloy MAR-M247 offers a satisfying combination of fatigue and creep properties and oxidation and corrosion resistance that are required for application at elevated temperatures in hostile environments. The microstructure consists mainly of the face centred cubic γ matrix and ordered γ´ strengthening precipitates (L12 crystal structure). The present work focuses on low cycle fatigue (LCF) behaviour of polycrystalline nickel-based superalloy MAR-M247 at high temperature. LCF tests were conducted on cylindrical specimens in a symmetrical push-pull cycle under strain control with constant total strain amplitude and strain rate at 700 °C in ambient air. Cyclic stress-strain curves and fatigue life curves in the representation of plastic strain amplitude vs. stress amplitude and stress amplitude vs. the number of cycles to failure, respectively, were plotted and compared with data obtained on Inconel 713LC. Special attention was paid to the investigation of crack initiation in MAR-M247 during low cycle fatigue. Crack initiation sites were studied by means of scanning electron microscopy (SEM) in dual beam microscope TESCAN LYRA 3 XMU FESEM equipped with focus ion beam (FIB). Specimens’ surface observations revealed the formation of pronounced surface relief indicating localisation of plastic deformation. Observations in transmission electron microscope (TEM) confirmed localisation of cyclic plastic deformation in persistent slip bands along {111} slip planes. Fractographic analysis revealed fatigue crack initiation sites. Fatigue crack propagation in stage I was typical of smooth facets up to 500 μm long.
Fatigue Crack Initiation in Nickel-Based Superalloy MAR-M247 at High Temperature
Šulák, Ivo ; Obrtlík, Karel
The present work is focused on the study of crack initiation during low cycle fatigue (LCF) loading of the second generation nickel-based superalloy MAR-M247 treated with hot isostatic pressing. LCF tests were conducted on cylindrical specimens in symmetrical push-pull cycle under strain control with constant total strain amplitude and strain rate at 800 °C in air atmosphere. Selected specimens were electrolytically polished to facilitate surface relief observations. Crack initiation sites were studied by means of scanning electron microscopy (SEM) in dual beam microscope TESCAN LYRA 3 XMU FESEM equipped with focus ion beam (FIB). The microstructure of the material is characterised by coarse dendritic grains with numerous carbides and small casting defects. The average grain size was 2.1 ± 0.3 mm. Fractographic analysis revealed the fatigue crack initiation sites and their relation to the casting defects and material microstructure. Casting defects, carbide inclusions and interdendritic areas were found to be important crack nucleation sites. Specimens’ surface observations revealed the formation of pronounced surface relief with short worm-like markings. Fatigue crack initiation in these places is documented and discussed.
Design elektronového mikroskopu
Švajdová, Anna ; Surman, Martin (oponent) ; Škaroupka, David (vedoucí práce)
Tématem diplomové práce je design skenovacího elektronového mikroskopu s fokusovaným iontovým svazkem. Práce se zabývá řešením designu krytů mikroskopu a přilehlého pracoviště operátora pro společnost Tescan Orsay Holding a.s.. Design je řešen jako první návrh směřující k budoucímu inovování designu celé produktové řady.

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