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Laboratory Separation of Methanol from the Azeotropic Mixture (25 wt% Methanol and 75 wt% trimethylborate.
Gaálová, Jana ; Vojtek, Lukáš ; Izák, Pavel
The work deals with laboratory separation of methanol from the azeotropic mixture (25 wt% methanol and 75 wt% trimethylborate). Four different manufactured membranes were tested. For all except one separation, separation was more or less successful. With PVA 4155-80 / 2871 the separation proceeded with good results, but very slowly, a condition that could increase the reaction rate could be an increase of temperature. Most selective membrane from Sulzer was PDMS 4155 -30/305 R, which separated MeOH with high efficiency and fast enough. The completely opposite effect than pervious membranes had the membrane PDMS 4060, which instead of MeOH separated Trimethylborate.

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