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National Repository of Grey Literature

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	The Effect of Experimental Design on Crystal Size of TiO2 Thin Films Prepared by Using Modified Supercritical Carbon Dioxide. Cerhová, Marie ; Sajfrtová, Marie ; Matějová, L. ; Dřínek, Vladislav ; Daniš, S. ; Jandová, Věra In this work, the method using pure and modified supercritical carbon dioxide was tested to prepare a set of crystalline TiO2 thin films deposited on soda-lime glass. Precursor solution for TiO2 films was prepared by a templated sol-gel method in the reverse micelle environment. Simple approach or combination of several steps performed at different temperature (40-150 °C) and solvent composition was applied at pressure 30 MPa. Water, ethanol and water : ethanol (1:1) mixture were added into supercritical CO2 as modifiers at concentration 10-30 wt.%. The effect of extraction design on microstructure and purity of TiO2 thin films were examined. Fulltext: content.csg - PDF Plný tet: SKMBT_C22016090211373 - PDF Detailed record
	Use of Supercritical Carbon Dioxide for Direct Preparation of Crystalline Monolithic TiO2 Aerogels. Cerhová, Marie ; Sajfrtová, Marie ; Matějová, L. ; Dřínek, Vladislav ; Daniš, S. ; Jandová, Věra The present work deals with the crystallization of monolithic TiO2 aerogels in environment of pure and water modified scCO2. To remove organic precursors used during sol-gel synthesis and to crystallize TiO2 the combination of several steps with pure and watermodified scCO2 was tested with respect the high porosity and the specific surface area of titania blocks. Fulltext: content.csg - PDF Plný tet: SKMBT_C22016090211380 - PDF Detailed record
	Preparation of Nanostructured Titania Thin Films Using Supercritical Carbon Dioxide Cerhová, Marie ; Sajfrtová, Marie ; Matějová, L. ; Dřínek, Vladislav ; Daniš, S. ; Jandová, Věra Extrakce čistým a modifikovaným superkritickým oxidem uhličitým (SFE) a extrakce podkritickou vodou byla využita k získání krystalických a čistých nanostrukturních tenkých filmů TiO2 a současně k odstranění organických prekurzorů ze syntézy solu sol-gel metodou. Při SFE byl sledován vliv teploty a použitého modifikátoru (vody, metanolu, etanolu a acetonu) na čistotu a mikrostrukturu tenkých filmů TiO2. Byl testován i kombinovaný postup extrakce, kdy se střídaly kroky s CO2 modifikovaným vodou a s CO2 modifikovaným organickými rozpouštědly. Čistota a krystalinita tenkých filmů byla zjištěna pomocí Ramanovy spektroskopie. Fázová složení a velikosti krystalů anatasu, žádané krystalické struktury, byly vyhodnoceny rentgenovou difrakční analýzou (XRD). Fulltext: content.csg - PDF Plný tet: SKMBT_C22015111812130 - PDF Detailed record

National Repository of Grey Literature : 23 records found   21 - 23  jump to record:

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4	Daniš, Stanislav

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