Original title:
Determination of Composition and Anomeric Ratio in Mixtures of Fluorinated Ologosaccharides.
Authors:
Červenková Šťastná, Lucie ; Kurfiřt, Martin ; Hamala, Vojtěch ; Karban, Jindřich Document type: Papers Conference/Event: Magnetic Moments in Central Europe 2019, Prague (CZ), 20190227
Year:
2019
Language:
eng Abstract:
Plenthora of glycosylation reactions was performed and sophisticated NMR approach for characteriza-tion of the coressponding products was aplied. ID 19F and *H NMR were utilized for accurate derermina-tion of anomeric ratios and 2D NMR techniques as HSQC, HMBC and COSY were used to assign the signals of individual anomers. In some cases, spectrum simulation was necessary to obtain the desired parameters.
Keywords:
2D NMR techniques; deoxofluorinated oligosaccharides; glycosylation Project no.: LM2015037 (CEP), GA17-18203S (CEP) Funding provider: GA MŠk Host item entry: Book of Abstracts, ISBN 978-80-86186-97-9
Rights: This work is protected under the Copyright Act No. 121/2000 Coll.